7BUV
Eucommia ulmoides TPT3, crystal form 2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL44XU |
| Synchrotron site | SPring-8 |
| Beamline | BL44XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-12-11 |
| Detector | RAYONIX MX300HE |
| Wavelength(s) | 0.9 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 234.386, 131.060, 103.924 |
| Unit cell angles | 90.00, 111.98, 90.00 |
Refinement procedure
| Resolution | 48.190 - 3.300 |
| R-factor | 0.2828 |
| Rwork | 0.282 |
| R-free | 0.30430 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4kk2 |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.785 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.190 | 3.418 |
| High resolution limit [Å] | 3.300 | 3.300 |
| Number of reflections | 43925 | 4399 |
| <I/σ(I)> | 14.96 | |
| Completeness [%] | 99.8 | |
| Redundancy | 5.8 | |
| CC(1/2) | 0.999 | 0.660 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 3350, DL-Malic acid, Risedronate, MgCl2 |
