7BTA
Crystal structure of Rheb D60K mutant bound to GDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-06-23 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 0.9792 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 108.860, 47.800, 61.070 |
Unit cell angles | 90.00, 112.75, 90.00 |
Refinement procedure
Resolution | 31.852 - 2.600 |
R-factor | 0.1936 |
Rwork | 0.191 |
R-free | 0.25590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1xtq |
RMSD bond length | 0.009 |
RMSD bond angle | 1.165 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.852 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.074 | 0.593 |
Number of reflections | 9007 | 679 |
<I/σ(I)> | 14.1 | 2.5 |
Completeness [%] | 97.8 | |
Redundancy | 4 | |
CC(1/2) | 0.998 | 0.881 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 8 | 290 | 0.2 M NaH2PO4: 16% PEG 3350 |