7BIK
Crystal structure of YTHDF2 in complex with m6Am
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-03-16 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1 |
Spacegroup name | P 65 |
Unit cell lengths | 80.368, 80.368, 113.769 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.050 - 2.100 |
R-factor | 0.1854 |
Rwork | 0.183 |
R-free | 0.22570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wqn |
RMSD bond length | 0.007 |
RMSD bond angle | 0.895 |
Data reduction software | XDS (March 15, 2019) |
Data scaling software | XSCALE (March 15, 2019) |
Phasing software | PHASER (1.19_4080) |
Refinement software | PHENIX (1.19_4080) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 44.050 | 44.050 | 2.230 |
High resolution limit [Å] | 2.100 | 6.240 | 2.100 |
Rmeas | 0.084 | 0.033 | 0.743 |
Number of reflections | 47916 | 1814 | 7675 |
<I/σ(I)> | 19.73 | 59.53 | 3.24 |
Completeness [%] | 100.0 | 99.7 | 99.7 |
Redundancy | 6.9 | ||
CC(1/2) | 0.999 | 0.999 | 0.861 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 277.15 | 2 M ammonium sulphate, 0.1 M Sodium citrate tribasic pH 5.6 |