7BI4
PI3KC2a core apo
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-15 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9184 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 135.193, 151.570, 56.044 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.060 - 2.420 |
R-factor | 0.2316 |
Rwork | 0.229 |
R-free | 0.27680 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7bi2 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.060 | 2.510 |
High resolution limit [Å] | 2.420 | 2.420 |
Rmeas | 0.122 | |
Number of reflections | 44453 | 6969 |
<I/σ(I)> | 10.55 | |
Completeness [%] | 99.8 | 97.4 |
Redundancy | 4.4 | |
CC(1/2) | 0.998 | 0.279 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 298 | 0.1MTris, 8-6% PEG3350, 0.2-0.1M MgSO4 |