7B6S
Sheep Polyomavirus VP1 in complex with 10 mM Forssman antigen pentaose
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 93 |
| Detector technology | PIXEL |
| Collection date | 2019-08-17 |
| Detector | DECTRIS PILATUS 2M-F |
| Wavelength(s) | 1.0077 |
| Spacegroup name | P 31 |
| Unit cell lengths | 130.494, 130.494, 222.435 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 42.714 - 1.923 |
| Rwork | 0.149 |
| R-free | 0.17570 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6y61 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.643 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 42.720 | 1.960 |
| High resolution limit [Å] | 1.850 | 1.850 |
| Rmeas | 0.105 | 1.045 |
| Number of reflections | 361163 | 57845 |
| <I/σ(I)> | 14.42 | 1.77 |
| Completeness [%] | 99.8 | 98.8 |
| Redundancy | 6.75 | 6.01 |
| CC(1/2) | 0.998 | 0.990 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | KSCN, PEG 3350 |
