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7B56

Crystal structure of CaMKII-actinin complex bound to AMPPNP

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04-1
Synchrotron siteDiamond
BeamlineI04-1
Temperature [K]100
Detector technologyPIXEL
Collection date2020-03-01
DetectorDECTRIS PILATUS3 S 6M
Wavelength(s)0.9119
Spacegroup nameP 21 21 21
Unit cell lengths64.426, 72.510, 92.001
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution52.770 - 1.450
R-factor0.1908
Rwork0.190
R-free0.21540
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2vz6
RMSD bond length0.006
RMSD bond angle0.974
Data reduction softwareDIALS
Data scaling softwareAimless
Phasing softwareMOLREP
Refinement softwarePHENIX (1.18.2_3874)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]92.0001.470
High resolution limit [Å]1.4501.450
Rpim0.0160.522
Number of reflections770653786
<I/σ(I)>18.5
Completeness [%]100.0
Redundancy12.1
CC(1/2)0.9990.825
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2770.1 M MES pH 6.0, 20% w/v PEG4000, 0.2 M Lithium Sulfate

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