7AU7
Crystal structure of Nod Factor Perception ectodomain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-3 |
Synchrotron site | MAX II |
Beamline | I911-3 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-05-10 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 77.410, 98.160, 71.890 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.080 - 2.547 |
R-factor | 0.2112 |
Rwork | 0.205 |
R-free | 0.26620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ebz |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.080 | 2.620 |
High resolution limit [Å] | 2.547 | 2.547 |
Rmerge | 0.155 | |
Rmeas | 0.168 | |
Number of reflections | 9247 | 136 |
<I/σ(I)> | 10.7 | 1.95 |
Completeness [%] | 79.6 | 20 |
Redundancy | 6.74 | |
CC(1/2) | 0.996 | 0.636 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 292.15 | 0.2 M Na-acetate * 3H2O, 0.1 M Na-cacodylate pH 6.5, 30% (w/v) PEG-8000, |