7A90
WT STING in complex with 3',3'-c-di[2'FdAM(PS)]
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-07-27 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 1.54 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 110.811, 110.811, 35.601 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.040 - 3.185 |
R-factor | 0.2193 |
Rwork | 0.217 |
R-free | 0.25070 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ksy |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER (2.8.2) |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.042 | 3.299 |
High resolution limit [Å] | 3.185 | 3.185 |
Number of reflections | 4032 | 390 |
<I/σ(I)> | 5.84 | 1.91 |
Completeness [%] | 99.8 | |
Redundancy | 11.6 | |
CC(1/2) | 0.967 | 0.678 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.2 M tri-Potassium Citrate monohydrate, 20% (w/v) PEG 3350, 0.1 M Natrium Citrate, 50 mM EDTA |