7WX1
E40K/M117L variant of Cu/Zn-superoxide dismutase from dog (Canis familiaris)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-08-22 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.275 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.511, 50.170, 185.751 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.480 - 1.650 |
R-factor | 0.2324 |
Rwork | 0.231 |
R-free | 0.26201 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.522 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | CRANK2 |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.430 | 1.740 |
High resolution limit [Å] | 1.650 | 1.650 |
Number of reflections | 43243 | 6108 |
<I/σ(I)> | 18.5 | |
Completeness [%] | 99.8 | |
Redundancy | 18.8 | |
CC(1/2) | 1.000 | 0.744 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 20% PEG 3350, 0.2M Sodium malonate, pH 7.0 |