7U3Q

[4T7] Self-assembling tensegrity triangle with four turns of DNA per axis with R3 symmetry

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-07-18
Detector	DECTRIS EIGER2 X 9M
Wavelength(s)	1.00743
Spacegroup name	H 3
Unit cell lengths	205.696, 205.696, 197.198
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	44.060 - 9.320
R-factor	0.095
Rwork	0.095
R-free	0.10020
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3gbi
RMSD bond length	0.015
RMSD bond angle	1.272
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.18.2_3874)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	86.266	86.266	10.244
High resolution limit [Å]	9.319	20.325	9.319
Number of reflections	1708	188	188
<I/σ(I)>	7.7
Completeness [%]	86.0
Redundancy	10.7	10.1	11.8
CC(1/2)	1.000	1.000	0.124

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	277	100 mM MOPS, 125 mM magnesium sulfate, sodium hydroxide