7SVO
DPP8 IN COMPLEX WITH LIGAND ICeD-1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-02-03 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9998 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 162.816, 246.016, 261.767 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 135.770 - 2.580 |
| R-factor | 0.1804 |
| Rwork | 0.180 |
| R-free | 0.20760 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6eoo |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.742 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 135.780 | 2.830 |
| High resolution limit [Å] | 2.580 | 2.580 |
| Rmerge | 0.065 | 0.596 |
| Number of reflections | 159983 | 38954 |
| <I/σ(I)> | 2.23 | |
| Completeness [%] | 97.5 | 98.7 |
| Redundancy | 3.9 | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.46 M Nacitrate pH 6.75 |
