7R6V

Human EXOG complexed with dRP-containing DNA

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-ID
Synchrotron site	APS
Beamline	19-ID
Temperature [K]	100
Detector technology	CCD
Collection date	2018-06-01
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.0
Spacegroup name	P 1
Unit cell lengths	73.749, 79.085, 79.635
Unit cell angles	69.05, 65.02, 89.72

Refinement procedure

Resolution	50.000 - 2.160
Rwork	0.200
R-free	0.24000
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5t5c
RMSD bond length	0.004
RMSD bond angle	0.679
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX (1.17)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.500
High resolution limit [Å]	2.160	2.160
Number of reflections	79362	7224
<I/σ(I)>	1.5
Completeness [%]	97.0
Redundancy	1.8
CC(1/2)	0.750	0.500

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		292	28% PEG 4K, 0.2 M Ammonium Sulphate, 0.1 M Na Acetate Trihydrate pH 4.6