7PA9

JC polyomavirus VP1 in complex with Fab 98D3

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	93
Detector technology	PIXEL
Collection date	2015-11-05
Detector	DECTRIS PILATUS 2M
Wavelength(s)	0.999990
Spacegroup name	P 21 21 21
Unit cell lengths	170.970, 202.310, 251.660
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.153 - 2.750
Rwork	0.207
R-free	0.26280
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3nxg 5bvj
RMSD bond length	0.006
RMSD bond angle	1.676
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	REFMAC (5.8.0258)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.850
High resolution limit [Å]	2.750	2.750
Number of reflections	225685	16539
<I/σ(I)>	11.99
Completeness [%]	100.0
Redundancy	13.8
CC(1/2)	0.990	0.680

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	277.15	0.1 M Ammonium tartrate dibasic pH 7.0, 12% (w/v) PEG 3350