Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-03-21 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9999 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 28.810, 153.730, 75.850 |
| Unit cell angles | 90.00, 100.33, 90.00 |
Refinement procedure
| Resolution | 38.462 - 1.650 |
| Rwork | 0.175 |
| R-free | 0.19920 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 7oao |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.337 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.000 | 1.690 |
| High resolution limit [Å] | 1.650 | 1.650 |
| Rpim | 0.044 | 0.560 |
| Number of reflections | 77705 | 5819 |
| <I/σ(I)> | 10 | 1.2 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 6.6 | 6 |
| CC(1/2) | 1.000 | 0.600 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M Ammonium fluoride and 20 % Peg 3350 |
