7NFT
Fujian capbinding domain in complex with Nb8208
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-05-14 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 6 |
Unit cell lengths | 128.195, 128.195, 70.266 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 70.270 - 3.140 |
R-factor | 0.2463 |
Rwork | 0.244 |
R-free | 0.29140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6s5v |
RMSD bond length | 0.002 |
RMSD bond angle | 0.498 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.1_4122) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 70.270 | 3.256 |
High resolution limit [Å] | 3.140 | 3.144 |
Number of reflections | 10820 | 377 |
<I/σ(I)> | 9.85 | |
Completeness [%] | 92.9 | |
Redundancy | 2 | |
CC(1/2) | 0.989 | 0.595 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% w/v PEG3350, 1 M (NH4)2SO4, 0.1M BIS-TRIS propane pH 5.5 |