7DNG
DARPin 63_B7 in complex with linear V3-crown (MN) peptide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-10-25 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1 |
Spacegroup name | P 64 |
Unit cell lengths | 94.530, 94.530, 39.370 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.930 - 1.420 |
R-factor | 0.1789 |
Rwork | 0.178 |
R-free | 0.20520 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1SVX chain A |
RMSD bond length | 0.004 |
RMSD bond angle | 0.612 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.930 | 1.471 |
High resolution limit [Å] | 1.420 | 1.420 |
Rmerge | 0.105 | 6.440 |
Rmeas | 0.110 | |
Number of reflections | 38156 | 3784 |
<I/σ(I)> | 13.72 | |
Completeness [%] | 100.0 | 99.92 |
Redundancy | 12.1 | 11.9 |
CC(1/2) | 1.000 | 0.117 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 30% Jeffamine ED-2001, 0.1M HEPES pH 7.0 |