7BDE
HUMAN BCL6 BTB-DOMAIN IN COMPLEX WITH GSK137
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-08-23 |
Detector | RIGAKU SATURN A200 |
Wavelength(s) | 1.541780 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 49.251, 49.251, 124.409 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.044 |
R-factor | 0.1834 |
Rwork | 0.180 |
R-free | 0.24100 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | IN-HOUSE DERIVED |
RMSD bond length | 0.006 |
RMSD bond angle | 1.409 |
Data reduction software | Aimless (0.7.4) |
Data scaling software | STARANISO (2.2.19) |
Phasing software | REFMAC (5.8.0253) |
Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.347 | 2.249 |
High resolution limit [Å] | 2.044 | 2.044 |
Rmerge | 0.167 | 2.195 |
Rmeas | 2.314 | |
Rpim | 0.717 | |
Number of reflections | 7572 | 379 |
<I/σ(I)> | 11 | 1.5 |
Completeness [%] | 64.9 | 13.3 |
Redundancy | 10.4 | 10 |
CC(1/2) | 0.784 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | PEG3350, Glycerol, BisTris Propane |