7AFW
Beta-Catenin in complex with compound 6
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SEALED TUBE |
| Source details | RIGAKU MICROMAX-003 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-11-27 |
| Detector | RIGAKU |
| Wavelength(s) | 1.541800 |
| Spacegroup name | P 3 2 1 |
| Unit cell lengths | 53.453, 53.453, 87.545 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 87.550 - 1.814 |
| R-factor | 0.2299 |
| Rwork | 0.227 |
| R-free | 0.28130 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3sla |
| RMSD bond length | 0.009 |
| RMSD bond angle | 0.970 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC (1.1.7) |
| Refinement software | BUSTER (2.11.7) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 87.545 | 1.929 |
| High resolution limit [Å] | 1.814 | 1.814 |
| Rmerge | 0.075 | 0.825 |
| Number of reflections | 11045 | 1066 |
| <I/σ(I)> | 24.6 | 1 |
| Completeness [%] | 80.9 | 24.5 |
| Redundancy | 8.3 | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 278 | 25% PEG 3350, 100 mM BIS-TRIS buffer pH 5.5 and 0.2 M Magnesium chloride |
