6Z90
Crystal structure of MINDY1 mutant-P138A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-14 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97625 |
Spacegroup name | P 41 2 2 |
Unit cell lengths | 98.649, 98.649, 166.073 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.000 - 3.590 |
R-factor | 0.2139 |
Rwork | 0.212 |
R-free | 0.25810 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5jkn |
RMSD bond length | 0.006 |
RMSD bond angle | 1.670 |
Data reduction software | XDS |
Data scaling software | Aimless (0.7.4) |
Phasing software | MoRDa |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.280 | 3.930 |
High resolution limit [Å] | 3.590 | 3.590 |
Rmerge | 0.094 | 1.037 |
Rmeas | 0.100 | 1.101 |
Rpim | 0.034 | 0.368 |
Total number of observations | 86341 | |
Number of reflections | 10152 | 2353 |
<I/σ(I)> | 12.5 | |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 8.5 | 8.8 |
CC(1/2) | 0.999 | 0.905 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293.15 | 0.7 M sodium citrate tribasic dihydrate, 0.1 M BIS-TRIS propane pH 7.0 |