6Z3J
Repulsive Guidance Molecule B (RGMB) in complex with Growth Differentiation Factor 5 (GDF5) (crystal form 1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-10-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9762 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 36.480, 127.750, 39.910 |
Unit cell angles | 90.00, 99.32, 90.00 |
Refinement procedure
Resolution | 39.380 - 1.650 |
R-factor | 0.1921 |
Rwork | 0.191 |
R-free | 0.21930 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6z3h |
RMSD bond length | 0.005 |
RMSD bond angle | 0.855 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13rc2_2986: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.380 | 1.690 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.088 | |
Number of reflections | 43071 | 3117 |
<I/σ(I)> | 9.5 | 0.5 |
Completeness [%] | 99.7 | |
Redundancy | 6.8 | |
CC(1/2) | 0.212 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 294 | 0.2 M Li2SO4, 0.1 M HEPES pH 7.5, 25% v/v PEG 3350. |