Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-02 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 119.318, 119.318, 114.758 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 59.730 | 3.180 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 1.677 | |
Number of reflections | 10169 | 1599 |
<I/σ(I)> | 17.1 | 1.7 |
Completeness [%] | 100.0 | |
Redundancy | 19.2 | |
CC(1/2) | 0.999 | 0.932 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.9 | 293.15 | 100 mM Sodium citrate, 0.2 M Ammonium Acetate and 3% MPD |