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6YXQ

Crystal structure of a DNA repair complex ASCC3-ASCC2

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsBESSY BEAMLINE 14.1
Synchrotron siteBESSY
Beamline14.1
Temperature [K]100
Detector technologyPIXEL
Collection date2018-11-20
DetectorDECTRIS PILATUS3 S 6M
Wavelength(s)0.97957
Spacegroup nameI 4
Unit cell lengths158.108, 158.108, 69.365
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution41.960 - 2.700
R-factor0.2063
Rwork0.204
R-free0.24740
Structure solution methodSAD
RMSD bond length0.007
RMSD bond angle0.907
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareAutoSol
Refinement softwarePHENIX (1.17.1_3660)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]41.9642.860
High resolution limit [Å]2.7002.700
Rmerge0.164
Number of reflections458457271
<I/σ(I)>5.89
Completeness [%]99.0
Redundancy3.5
CC(1/2)0.9950.139
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP277.15MES-NaOH, pH 6.5, polyethylene glycol 3350, 2-methyl-2,4-pentanediol and methanol

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