6YTI
CLK1 bound with ETH1610 (Cpd 17)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-03-23 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 91.518, 63.873, 79.410 |
Unit cell angles | 90.00, 118.83, 90.00 |
Refinement procedure
Resolution | 48.030 - 2.400 |
R-factor | 0.1982 |
Rwork | 0.195 |
R-free | 0.25550 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1z57 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.689 |
Data reduction software | XDS |
Data scaling software | Aimless (0.7.4) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.030 | 47.980 | 2.490 |
High resolution limit [Å] | 2.400 | 8.980 | 2.400 |
Rmerge | 0.153 | 0.034 | 1.064 |
Rmeas | 0.166 | 0.037 | 1.149 |
Rpim | 0.062 | 0.014 | 0.433 |
Total number of observations | 2249 | 11317 | |
Number of reflections | 15727 | 325 | 1633 |
<I/σ(I)> | 10.1 | 39.4 | 1.9 |
Completeness [%] | 99.4 | 99.3 | 98.9 |
Redundancy | 7 | 6.9 | 6.9 |
CC(1/2) | 0.996 | 0.999 | 0.707 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9.3 | 277 | 29% PEG 6k, 0.1M bicine |