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6YFZ

Crystal structure of MKK7 (MAP2K7), apo form

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]100
Detector technologyPIXEL
Collection date2014-10-04
DetectorDECTRIS PILATUS3 6M
Wavelength(s)1.02823
Spacegroup nameP 21 21 21
Unit cell lengths57.460, 74.451, 81.770
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution30.410 - 1.900
R-factor0.1944
Rwork0.192
R-free0.23730
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2dyl
RMSD bond length0.016
RMSD bond angle1.678
Data reduction softwareiMOSFLM
Data scaling softwareSCALA (3.3.21)
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0103)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]30.41030.4082.000
High resolution limit [Å]1.9006.0101.900
Rmerge0.1030.0440.843
Rmeas0.1130.0480.922
Rpim0.0450.0200.367
Number of reflections282209984047
<I/σ(I)>9.210.80.9
Completeness [%]99.698.699.6
Redundancy6.15.66.1
CC(1/2)0.9960.621
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.8277.1519% PEG3350, 0.15 M ammonium acetate, 0.1 M tris, pH 7.8

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