6YF0
FKBP12 in complex with the BMP potentiator compound 9 at 1.55 A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-02-04 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.99996 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 62.338, 62.338, 135.408 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.540 - 1.550 |
R-factor | 0.2378 |
Rwork | 0.237 |
R-free | 0.25710 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4dh0 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.107 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.540 | 1.590 |
High resolution limit [Å] | 1.550 | 1.550 |
Rmerge | 0.038 | 1.058 |
Rmeas | 0.040 | 1.086 |
Rpim | 0.917 | |
Number of reflections | 23333 | 1596 |
<I/σ(I)> | 43.6 | 3.6 |
Completeness [%] | 99.7 | 100 |
Redundancy | 18.8 | 19.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | 2.2 M AmSO4, 0.2 M NaThiocyanate |