6YD6
SaFtsZ-UCM152 (comp.20)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-03-17 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97918 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 71.744, 50.184, 88.374 |
Unit cell angles | 90.00, 111.06, 90.00 |
Refinement procedure
Resolution | 40.160 - 1.700 |
R-factor | 0.1667 |
Rwork | 0.165 |
R-free | 0.20040 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3v0a |
RMSD bond length | 0.010 |
RMSD bond angle | 1.141 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.160 | 1.770 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.030 | 0.300 |
Rmeas | 0.040 | 0.430 |
Rpim | 0.030 | 0.300 |
Number of reflections | 31638 | 3192 |
<I/σ(I)> | 9.8 | 2.03 |
Completeness [%] | 97.4 | |
Redundancy | 3 | |
CC(1/2) | 0.990 | 0.820 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 25% PEG5K MME, 10% EthGly, 0.2 M Li2SO4, 0.1 M Tris pH 8.5 |