6YBH

Deoxyribonucleoside Kinase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RUH3R
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2019-07-17
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.5418
Spacegroup name	H 3
Unit cell lengths	190.929, 190.929, 115.461
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	42.660 - 2.400
R-factor	0.2083
Rwork	0.206
R-free	0.26250
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2vp0
RMSD bond length	0.010
RMSD bond angle	1.630
Data reduction software	MOSFLM
Data scaling software	SCALEPACK
Phasing software	PHASER
Refinement software	REFMAC (5.8.0258)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.660	2.486
High resolution limit [Å]	2.400	2.400
Number of reflections	61274	6142
<I/σ(I)>	40.13
Completeness [%]	99.8
Redundancy	14.8
CC(1/2)	0.799	0.670

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5.6	298	0.1M KNa Tarta