6Y95
Ca2+-free Calmodulin mutant N53I
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE III | 600 | |
| 2 | Bruker | AVANCE III | 800 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D 1H-15N HSQC |
| 10 | 1 | 1 | 3D HBHA(CO)NH |
| 11 | 2 | 2 | 15N-T2 |
| 12 | 2 | 2 | 15N-T1 |
| 13 | 2 | 2 | T2-relaxation dispersion |
| 14 | 2 | 2 | {1H}-15N-NOE |
| 15 | 3 | 3 | T2-relaxation dispersion |
| 16 | 3 | 3 | {1H}-15N-NOE |
| 17 | 3 | 3 | 15N-T2 |
| 18 | 3 | 3 | 15N-T1 |
| 19 | 1 | 1 | 3D HCCH-TOCSY |
| 2 | 1 | 2 | 2D 1H-13C HSQC aliphatic |
| 3 | 1 | 1 | 2D 1H-13C HSQC aromatic |
| 4 | 1 | 1 | 3D HNCA |
| 5 | 1 | 1 | 3D CBCA(CO)NH |
| 6 | 1 | 1 | 3D 1H-13C NOESY aromatic |
| 7 | 1 | 1 | 3D 1H-13C NOESY aliphatic |
| 8 | 1 | 1 | 3D 1H-15N NOESY |
| 9 | 1 | 1 | 3D HCCH-TOCSY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.3 | 1 | 298.1 |
| 2 | 6.56 | 1 | 298.1 |
| 3 | 6.53 | 1 | 298.1 |
Conformers
| Conformers Calculated Total Number | 30 |
| Conformers Submitted Total Number | 20 |
