6Y60
Structure of Human Polyomavirus 12 VP1 in complex with 3'-Sialyllactosamine
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2013-06-27 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.00 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 83.322, 141.724, 251.302 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.370 - 1.798 |
Rwork | 0.203 |
R-free | 0.24300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4fmg |
RMSD bond length | 0.009 |
RMSD bond angle | 1.629 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.370 | 1.910 |
High resolution limit [Å] | 1.798 | 1.798 |
Rmeas | 0.125 | 1.770 |
Number of reflections | 274251 | 42872 |
<I/σ(I)> | 12.21 | 1.34 |
Completeness [%] | 99.4 | |
Redundancy | 7.04 | |
CC(1/2) | 0.999 | 0.725 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | Ammonium acetate, Bis-Tris, 2-methyl-2,4-pentanediol |