6XVM
Crystal structure of c-Src SH3 domain without ATCUN motif: monomer 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-03-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.610, 52.519, 45.589 |
Unit cell angles | 90.00, 90.01, 90.00 |
Refinement procedure
Resolution | 40.610 - 0.900 |
R-factor | 0.1394 |
Rwork | 0.139 |
R-free | 0.14950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4jz4 |
Data reduction software | XDS |
Data scaling software | Aimless (0.7.4) |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 40.610 | 40.610 | 0.920 |
High resolution limit [Å] | 0.900 | 4.930 | 0.900 |
Rmerge | 0.040 | 0.040 | 0.180 |
Rmeas | 0.045 | 0.046 | 0.246 |
Rpim | 0.021 | 0.021 | 0.166 |
Total number of observations | 2883 | 4619 | |
Number of reflections | 257512 | 686 | 2811 |
<I/σ(I)> | 16.2 | 20.2 | 6.5 |
Completeness [%] | 92.5 | 76.6 | 40.2 |
Redundancy | 3.9 | 4.2 | 1.6 |
CC(1/2) | 0.998 | 0.996 | 0.913 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 298 | 3M ammonium sulfate, 0.1 M MES |