6XUO
mature recombinant horse NGF
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 90 |
Detector technology | PIXEL |
Collection date | 2016-04-02 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9184 |
Spacegroup name | I 21 3 |
Unit cell lengths | 108.490, 108.490, 108.490 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.245 - 2.803 |
R-factor | 0.2238 |
Rwork | 0.219 |
R-free | 0.26610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1sg1 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 76.710 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.072 | 0.858 |
Rmeas | 0.074 | 0.884 |
Rpim | 0.018 | 0.212 |
Number of reflections | 5381 | 776 |
<I/σ(I)> | 24.8 | 3.6 |
Completeness [%] | 100.0 | 100 |
Redundancy | 17.5 | 17 |
CC(1/2) | 1.000 | 0.799 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 0.11 M Zn acetate, 0.1 M MES (pH 6.5) |