6XLW
Crystal structure of U2AF65 bound to AdML splice site sequence
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-06-28 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.033 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.398, 62.731, 77.427 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.710 - 1.500 |
R-factor | 0.1326 |
Rwork | 0.131 |
R-free | 0.15350 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.008 |
RMSD bond angle | 1.038 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.8) |
Phasing software | PHENIX |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.710 | 1.520 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.053 | 0.098 |
Rpim | 0.032 | 0.062 |
Number of reflections | 33522 | 1417 |
<I/σ(I)> | 22.3 | 9.9 |
Completeness [%] | 97.0 | 85 |
Redundancy | 6.9 | 6 |
CC(1/2) | 0.998 | 0.991 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277.15 | 1M Succinic Acid, 0.1M HEPES pH 7, 3% PEG MME 2000 |