6WVD
Human JAGN1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-19 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9792 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 90.774, 42.718, 111.782 |
Unit cell angles | 90.00, 103.79, 90.00 |
Refinement procedure
Resolution | 38.440 - 2.250 |
R-factor | 0.1965 |
Rwork | 0.195 |
R-free | 0.22720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b3p |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.290 |
High resolution limit [Å] | 2.250 | 6.100 | 2.250 |
Rmerge | 0.091 | 0.056 | 0.607 |
Rmeas | 0.110 | 0.068 | 0.741 |
Rpim | 0.062 | 0.037 | 0.418 |
Number of reflections | 19195 | 1009 | 898 |
<I/σ(I)> | 8.8 | ||
Completeness [%] | 95.6 | 96 | 93.3 |
Redundancy | 2.8 | 2.9 | 2.7 |
CC(1/2) | 0.993 | 0.625 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 295 | 30% PEG400, 0.1 M Li2SO4, 0.1M NaCl, 0.1 M Tris pH 8.0 |