6WMZ
Crystal structure of human SFPQ/NONO complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-07-26 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.954 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 66.630, 112.940, 204.620 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 63.436 - 2.850 |
Rwork | 0.236 |
R-free | 0.28260 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wii |
RMSD bond length | 0.003 |
RMSD bond angle | 1.241 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 68.210 | 2.980 |
High resolution limit [Å] | 2.850 | 2.850 |
Number of reflections | 36690 | 4446 |
<I/σ(I)> | 10.2 | |
Completeness [%] | 99.5 | |
Redundancy | 4.7 | |
CC(1/2) | 0.996 | 0.627 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M Tris-HCl (pH 8.5), 0.2 M ammonium sulfate, 19% PEG 3350 |