6WIT
Crystal structure of NHP D15.SD7 Fab in complex with 16055 V1V2 1FD6 scaffold
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.1 |
Synchrotron site | ALS |
Beamline | 5.0.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-21 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.409, 89.809, 172.782 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.480 - 2.790 |
R-factor | 0.2282 |
Rwork | 0.224 |
R-free | 0.28360 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4rfo |
RMSD bond length | 0.005 |
RMSD bond angle | 0.747 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.17.1_3660: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.481 | 2.850 |
High resolution limit [Å] | 2.790 | 2.800 |
Rmerge | 0.144 | 0.927 |
Rmeas | 0.125 | 0.495 |
Rpim | 0.049 | 0.573 |
Number of reflections | 28183 | 1436 |
<I/σ(I)> | 16.05 | 1.47 |
Completeness [%] | 95.7 | 66.75 |
Redundancy | 6.2 | 4.2 |
CC(1/2) | 0.992 | 0.573 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 0.2 M ammonium sulfate, 0.1 M MES, pH 6.5, 22% PEG8000 |