6VSK
Crystal structure of the P-Rex1 DEP1 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2018-11-02 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0332 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 103.152, 103.152, 67.981 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.620 - 3.120 |
R-factor | 0.1855 |
Rwork | 0.183 |
R-free | 0.23320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1o7f |
RMSD bond length | 0.009 |
RMSD bond angle | 1.796 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.170 |
High resolution limit [Å] | 3.120 | 3.120 |
Rmeas | 0.152 | 0.602 |
Rpim | 0.049 | 0.316 |
Number of reflections | 4105 | 185 |
<I/σ(I)> | 19 | 1.3 |
Completeness [%] | 99.3 | 95.4 |
Redundancy | 8.4 | 3 |
CC(1/2) | 0.713 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293.15 | 0.1 M HEPES, pH 6.5, 45% w/v poly(acrylic acid sodium salt)2100 |