6VOU
Aminoglycoside N-2'-Acetyltransferase-Ia [AAC(2')-Ia] in complex with acetylated-plazomicin and CoA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-08-15 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97857 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 73.510, 73.510, 147.120 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 63.660 - 1.950 |
R-factor | 0.1935 |
Rwork | 0.192 |
R-free | 0.22490 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.006 |
RMSD bond angle | 0.948 |
Data reduction software | XDS |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 63.660 | 2.020 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.052 | |
Rmeas | 0.055 | |
Rpim | 0.018 | |
Number of reflections | 33925 | 3293 |
<I/σ(I)> | 18.89 | |
Completeness [%] | 98.8 | |
Redundancy | 8.1 | |
CC(1/2) | 0.999 | 0.718 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277.15 | acetyl CoA, plazomicin, LiCl, MPD |