6VNP
Crystal structure of DPO4 extension past 8-oxoadenine (oxoA) and dT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 120 |
Detector technology | PIXEL |
Collection date | 2018-11-28 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1 |
Spacegroup name | P 1 |
Unit cell lengths | 53.255, 98.984, 102.875 |
Unit cell angles | 90.03, 89.99, 89.92 |
Refinement procedure
Resolution | 47.300 - 2.420 |
Rwork | 0.199 |
R-free | 0.24160 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jx4 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.271 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX (1.17) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.470 |
High resolution limit [Å] | 2.420 | 2.420 |
Rpim | 0.061 | 0.454 |
Number of reflections | 78571 | 4003 |
<I/σ(I)> | 8.1 | |
Completeness [%] | 97.6 | |
Redundancy | 1.9 | |
CC(1/2) | 0.644 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 50 mM Tris 7.5 20% PEG3350 100 mM Magnesium Acetate |