6VK8
Crystal Structure of Methylosinus trichosporium OB3b Soluble Methane Monooxygenase Hydroxylase and Regulatory Component Complex with small organic carboxylate at active center
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-07 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 101.866, 105.349, 297.720 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 85.990 - 2.030 |
R-factor | 0.1688 |
Rwork | 0.167 |
R-free | 0.20750 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.007 |
RMSD bond angle | 0.836 |
Data reduction software | XDS |
Data scaling software | PHENIX |
Phasing software | PHENIX |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 101.870 | 2.100 |
High resolution limit [Å] | 2.030 | 2.030 |
Rmerge | 0.137 | |
Rpim | 1.105 | |
Number of reflections | 203307 | 19824 |
<I/σ(I)> | 7.9 | |
Completeness [%] | 98.5 | |
Redundancy | 4.1 | |
CC(1/2) | 0.994 | 0.387 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | Tacsimate, PEG3350 |