6VCQ
Crystal structure of E.coli RppH in complex with GTP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2012-08-13 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 60.671, 60.671, 74.265 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.180 - 1.600 |
R-factor | 0.1748 |
Rwork | 0.173 |
R-free | 0.20640 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4s2y |
RMSD bond length | 0.006 |
RMSD bond angle | 0.940 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.16_3546) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.180 | 1.700 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 39944 | 6148 |
<I/σ(I)> | 14.4 | |
Completeness [%] | 99.1 | |
Redundancy | 3.8 | |
CC(1/2) | 0.999 | 0.672 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 0.4 M (NH4)2SO4 and 10% (v/v) PEG4000 |