6V7W
Crystal structure of LasR-Aqs1 complex from Pseudomonas aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 105 |
Detector technology | PIXEL |
Collection date | 2019-06-28 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97920 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 97.975, 100.438, 106.631 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 73.110 - 3.000 |
R-factor | 0.2515 |
Rwork | 0.250 |
R-free | 0.27180 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6v7u |
RMSD bond length | 0.002 |
RMSD bond angle | 0.604 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 73.110 | 3.038 |
High resolution limit [Å] | 3.000 | 3.000 |
Number of reflections | 21677 | |
<I/σ(I)> | 25.4 | |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 19.7 | |
CC(1/2) | 0.998 | 1.000 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2M sodium chloride, 0.1M HEPES:NaOH, pH 7.5 and 30% PEG400, 15% glycerol |