6UG7
Complex of ch28/11 Fab and SSEA-4 (tetragonal form)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-16 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.954 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 67.795, 67.795, 234.040 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.600 |
High resolution limit [Å] | 1.520 | 1.500 |
Rmeas | 0.100 | 0.480 |
Number of reflections | 84916 | 13419 |
<I/σ(I)> | 15.8 | |
Completeness [%] | 99.9 | |
Redundancy | 13.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 291 | PEG 4000, sodium acetate, ammonium sulfate |