6U6U
IL36R extracellular domain in complex with BI655130 Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-05-16 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.000000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 60.698, 70.663, 233.268 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.990 - 2.310 |
R-factor | 0.1802 |
Rwork | 0.179 |
R-free | 0.20210 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1g0y |
RMSD bond length | 0.009 |
RMSD bond angle | 1.087 |
Data reduction software | XDS |
Data scaling software | d*TREK |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 116.630 | 2.318 |
High resolution limit [Å] | 2.310 | 2.310 |
Rmerge | 0.090 | 0.921 |
Number of reflections | 45094 | 45094 |
<I/σ(I)> | 12.7 | 2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 6.7 | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.6 M Na3C6H5O7 |