Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

6TYP

KEAP1 Kelch domain in complex with Compound 2

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06DA
Synchrotron siteSLS
BeamlineX06DA
Temperature [K]100
Detector technologyPIXEL
Collection date2015-10-15
DetectorDECTRIS PILATUS 300K
Wavelength(s)0.98
Spacegroup nameC 1 2 1
Unit cell lengths125.792, 75.679, 48.648
Unit cell angles90.00, 106.81, 90.00
Refinement procedure
Resolution50.000 - 2.500
Rwork0.174
R-free0.21500
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4iqk
Data reduction softwareMOSFLM
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwarePHENIX
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.650
High resolution limit [Å]2.4902.490
Number of reflections15170786
<I/σ(I)>8.8
Completeness [%]99.7
Redundancy3.4
CC(1/2)0.9900.410
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP72893.0M sodium formate pH 7.0

221051

PDB entries from 2024-06-12

PDB statisticsPDBj update infoContact PDBjnumon