Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I23 |
| Synchrotron site | Diamond |
| Beamline | I23 |
| Temperature [K] | 80 |
| Detector technology | PIXEL |
| Collection date | 2019-08-02 |
| Detector | DECTRIS PILATUS 12M |
| Wavelength(s) | 2.755 |
| Spacegroup name | P 3 2 1 |
| Unit cell lengths | 148.204, 148.204, 45.652 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 128.348 - 2.350 |
| Rwork | 0.192 |
| R-free | 0.24530 |
| Structure solution method | SAD |
| Starting model (for MR) | 6fax |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.585 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | CRANK2 |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 128.350 | 2.430 |
| High resolution limit [Å] | 2.350 | 2.350 |
| Rmerge | 0.116 | |
| Rmeas | 0.129 | |
| Rpim | 0.036 | 0.771 |
| Number of reflections | 22283 | 1933 |
| <I/σ(I)> | 14.5 | 0.9 |
| Completeness [%] | 92.4 | 83.3 |
| Redundancy | 12 | 10.3 |
| CC(1/2) | 0.998 | 0.373 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | PEG 4000, cacodylate |
