6TGE
NADP dependent methylene-tetrahydromethanopterin dehydrogenase-NADP+-methenyl-H4MPT+ complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-11-28 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 |
Unit cell lengths | 98.640, 123.500, 167.300 |
Unit cell angles | 94.79, 100.39, 108.97 |
Refinement procedure
Resolution | 48.761 - 1.500 |
R-factor | 0.1871 |
Rwork | 0.186 |
R-free | 0.21630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1lu9 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.600 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 1110526 | 191566 |
<I/σ(I)> | 9.6 | |
Completeness [%] | 95.5 | |
Redundancy | 3.9 | |
CC(1/2) | 0.999 | 0.574 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 293 | 22% PEG4000, 0.2 M ammonium sulfate, 0.1 M sodium acetate |