6SEV
Structure of Dps from Listeria innocua soaked with 10 mM zinc for 120 minutes
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-01-01 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 84.831, 84.831, 267.358 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 2.020 - 2.000 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.100 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 2.300 | |
Number of reflections | 66812 | 10607 |
<I/σ(I)> | 15.6 | |
Completeness [%] | 99.7 | |
Redundancy | 16.2 | |
CC(1/2) | 0.990 | 0.330 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294 | 30% PEG1500, 100 mM Hepes pH 7.5 |