6SAK
Structure of the OTULINcat C129A - SNX27 PDZ domain complex.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 110 |
Detector technology | PIXEL |
Collection date | 2017-12-15 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.96861 |
Spacegroup name | P 1 |
Unit cell lengths | 54.645, 62.912, 72.017 |
Unit cell angles | 65.13, 85.98, 85.38 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.650 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.088 | 0.531 |
Number of reflections | 55998 | 7167 |
<I/σ(I)> | 5.7 | 1.7 |
Completeness [%] | 95.6 | |
Redundancy | 1.7 | |
CC(1/2) | 0.989 | 0.382 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.8 | 291 | 19% (w/v) PEG 3,350, 200 mM Li2(SO4), 100 mM Bis-Tris pH 6.8 |