6S5A
CRYSTAL STRUCTURE OF FC P329G LALA WITH ANTI FC P329G FAB
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 110 |
| Detector technology | PIXEL |
| Collection date | 2018-09-16 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.999 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 71.022, 135.545, 137.259 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 68.630 - 1.720 |
| R-factor | 0.197 |
| Rwork | 0.196 |
| R-free | 0.22600 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.070 |
| Data reduction software | XDS |
| Data scaling software | SADABS |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.7) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 68.630 | 1.810 |
| High resolution limit [Å] | 1.720 | 1.720 |
| Number of reflections | 140984 | 19727 |
| <I/σ(I)> | 3.5 | |
| Completeness [%] | 100.0 | |
| Redundancy | 7.49 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.04M potassium phosphate monobasic, 16% PEG8000, 20% Glycerol |
