6S08
Crystal Structure of Properdin (TSR domains N1 & 456)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-11-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9789 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 111.995, 114.860, 39.822 |
Unit cell angles | 90.00, 99.56, 90.00 |
Refinement procedure
Resolution | 79.610 - 2.030 |
R-factor | 0.2136 |
Rwork | 0.212 |
R-free | 0.24760 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.589 |
Data reduction software | DIALS |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 79.610 | 2.305 |
High resolution limit [Å] | 2.030 | 2.030 |
Rmerge | 0.161 | 1.249 |
Rmeas | 0.190 | 1.482 |
Rpim | 0.100 | 0.784 |
Number of reflections | 17424 | 871 |
<I/σ(I)> | 3.4 | 1.5 |
Completeness [%] | 54.5 | 8.7 |
Redundancy | 3.5 | 3.4 |
CC(1/2) | 0.982 | 0.469 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | Potassium Sulphate, PEG 3350 |